High temperature oxygen free oven
heating at a temperature of 3 5 ° C / min at room temperature for 40 minutes to 200 ° C constant temperature for 45 minutes at 200 ° C rise to 375 ° C in 40 min 375 ° C constant temperature 1H finally at a cooling rate of 3 5 ° C per minute from 375 ° C to 75 ° C in about 79 minutes Model